Machine learning discovery of novel antihypertensive peptides from highland barley protein inhibiting angiotensin I-converting enzyme (ACE).

Journal: Food research international (Ottawa, Ont.)
PMID:

Abstract

Hypertension is a major global health concern, and there is a need for new antihypertensive agents derived from natural sources. This study aims to identify novel angiotensin I-converting enzyme (ACE) inhibitors from bioactive peptides derived from food sources, particularly highland barley proteins, addressing the gap in effective natural ACE inhibitors. This research employs a machine learning-based pipeline combined with peptidomics to screen for ACE-inhibitory peptides, Gradient Boosted Decision Trees (GBDT) with the best performance among four tested models was used to predict the ACE-inhibitory capacity of peptides derived from papain-hydrolyzed highland barley protein. The selected peptides were validated through computer simulations and in vitro experiments, with FPRPFL identified as the most potent ACE-inhibitor (IC = 1.18 μM). Enzyme inhibition kinetics and digestion stability simulations were used to investigate its inhibition mode and stability. The binding mode and mechanism of action of FPRPFL with ACE were further analyzed using circular dichroism, molecular docking and molecular dynamics simulations. Network pharmacology revealed its multi-target and multi-pathway antihypertensive properties. The integration of machine learning and in vitro experiments enables accurate bioactive peptides identification and comprehensive their functionality analysis, establishing a valuable pipeline for elucidating peptide mechanisms and laying a solid foundation for industrial-scale production of natural ACE-inhibitors.

Authors

  • Xin Bao
    Hospital of Stomatology, Jilin University, 1500 Qinghua Road, Changchun 130021, China.
  • Yiyun Zhang
    National Engineering and Technology Research Center for Fruits and Vegetables, College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, PR China. Electronic address: 18681357759@163.com.
  • Liyang Wang
    Beijing Advanced Innovation Center for Food Nutrition and Human Health, College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, China.
  • Zijian Dai
    National Engineering and Technology Research Center for Fruits and Vegetables, College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, PR China. Electronic address: daizijian666@163.com.
  • Yiqing Zhu
    National Engineering and Technology Research Center for Fruits and Vegetables, College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, PR China.
  • Mengyao Huo
    National Engineering and Technology Research Center for Fruits and Vegetables, College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, PR China.
  • Rong Li
    Department of Neurology, People's Hospital of Longhua, Shenzhen, China.
  • Yichen Hu
    Key Laboratory of Coarse Cereal Processing, Ministry of Agriculture and Rural Affairs, School of Pharmacy, Key Laboratory of Medicinal and Edible Plants Resources Development of Sichuan Education Department, Sichuan Industrial Institute of Antibiotics, Chengdu University, Chengdu 610106, China.
  • Qun Shen
    National Engineering and Technology Research Center for Fruits and Vegetables, College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, PR China; National Center of Technology Innovation (Deep Processing of Highland Barley) in Food Industry, China Agricultural University, No. 17 Qinghua East Road, Haidian District, Beijing 100083, PR China. Electronic address: shenqun@cau.edu.cn.
  • Yong Xue
    Guangzhou Panyu Central Hospital, Guangzhou, China.