Harnessing near-infrared and Raman spectral sensing and artificial intelligence for real-time monitoring and precision control of bioprocess.

Journal: Bioresource technology
PMID:

Abstract

Effective monitoring and control of bioprocesses are critical for industrial biomanufacturing. This study demonstrates the integration of near-infrared and Raman spectroscopy for real-time monitoring and precise control of gentamicin fermentation. The orthogonal method reduced redundant features and improved spectral model performance by 9.2-100.4 % in terms of the coefficient of determination (R). The combinatorial spectral model outperformed single-source models in external validation (R > 0.99). An AI-based platform, combining dual-sensors data collection, ML-based prediction, and automated feeding control, was developed for fully automated fed-batch fermentation. This platform dynamically adjusted feeding rates, maintained low glucose concentrations (5 g/L) with accuracy and coefficient of variation below 2 %, and increased gentamicin C1a concentration (346.5 mg/L) by 33.0 % compared to traditional intermittent feeding. These findings underscore the transformative potential of combinatorial spectroscopy and machine learning for real-time bioprocess monitoring, offering a scalable solution for enhancing industrial fermentation efficiency and product titer.

Authors

  • Feng Xu
    Orthopedics Department of the First Affiliated Hospital of Tsinghua University, Beijing, China.
  • Lihuan Su
    State Key Laboratory of Bioreactor Engineering, Qingdao Innovation Institute of East China University of Science and Technology, East China University of Science and Technology, Shanghai, China.
  • Hao Gao
    Institute of Pharmaceutical Analysis , College of Pharmacy , Jinan University , Guangzhou , Guangdong 510632 , China . Email: haibo.zhou@jnu.edu.cn ; Email: jzjjackson@hotmail.com ; Email: tghao@jnu.edu.cn.
  • Yuan Wang
    State Key Laboratory of Soil and Sustainable Agriculture, Changshu National Agro-Ecosystem Observation and Research Station, Institute of Soil Science, Chinese Academy of Sciences, Nanjing, China.
  • Rong Ben
    State Key Laboratory of Bioreactor Engineering, Qingdao Innovation Institute of East China University of Science and Technology, East China University of Science and Technology, Shanghai, China.
  • Kaihao Hu
    State Key Laboratory of Bioreactor Engineering, Qingdao Innovation Institute of East China University of Science and Technology, East China University of Science and Technology, Shanghai, China.
  • Ali Mohsin
    State Key Laboratory of Bioreactor Engineering, East China University of Science and Technology, Shanghai, China.
  • Chao Li
    McGill University Health Centre, McGill Adult Unit for Congenital Heart Disease Excellence, Montreal, Québec, Canada.
  • Ju Chu
    State Key Laboratory of Bioreactor Engineering, East China University of Science and Technology, 130 Meilong Road, Shanghai, 200237, People's Republic of China.
  • Xiwei Tian
    State Key Laboratory of Bioreactor Engineering, East China University of Science and Technology, Shanghai, China.