Testing Precision Limits of Neural Network-Based Quality Control Metrics in High-Throughput Digital Microscopy.

Journal: Pharmaceutical research
PMID:

Abstract

OBJECTIVE: Digital microscopy is used to monitor particulates such as protein aggregates within biopharmaceutical products. The images that result encode a wealth of information that is underutilized in pharmaceutical process monitoring. For example, images of particles in protein drug products typically are analyzed only to obtain particle counts and size distributions, even though the images also reflect particle characteristics such as shape and refractive index. Multiple groups have demonstrated that convolutional neural networks (CNNs) can extract information from images of protein aggregates allowing assignment of the likely stress at the "root-cause" of aggregation. A practical limitation of previous CNN-based approaches is that the potential aggregation-inducing stresses must be known a priori, disallowing identification of particles produced by unknown stresses.

Authors

  • Christopher P Calderon
    Department of Chemical and Biological Engineering, Center for Pharmaceutical Biotechnology, University of Colorado Boulder, Boulder, Colorado.
  • Dean C Ripple
    Biomolecular Measurement Division, National Institute of Standards and Technology, Gaithersburg, MD, 20899, USA.
  • Charudharshini Srinivasan
    Division of Product Quality Research, Office of Testing and Research, OPQ, CDER, FDA, MD, 20993, USA.
  • Youlong Ma
    Division of Product Quality Research, Office of Testing and Research, OPQ, CDER, FDA, MD, 20993, USA.
  • Michael J Carrier
    Biomolecular Measurement Division, National Institute of Standards and Technology, Gaithersburg, MD, 20899, USA.
  • Theodore W Randolph
    Department of Chemical and Biological Engineering, Center for Pharmaceutical Biotechnology, University of Colorado Boulder, Boulder, Colorado 80309.
  • Thomas F O'Connor
    Division of Product Quality Research, Office of Testing and Research, OPQ, CDER, FDA, MD, 20993, USA.